Petrophysical properties of drill core and drill cuttings samples from both bore holes of the German Continental Deep Drilling Program (KTB) measured at atmospheric pressure and room temperature in the field laboratory are presented, along with data of core samples measured at simulated in situ conditions by other laboratories. Most of the petrophysical properties show a bimodal frequency distribution corresponding to the two main lithologies (gneiss and metabasite), except electrical resitivity and Th/U ratio which are lithology independent (monomodal distribution). Low resistivities are mainly associated with fractures zones enriched in fluids and graphite. The most abundant ferrimagnetic mineral is monoclinic pyrrhotite. Below 8600 m, hexagonal pyrrhotite with a Curie temperature of 260°C is the stable phase. Thus the Curie isotherm of the predominant pyrrhotite was reached (bottom hole temperature about 265°C). The highest values of magnetic susceptibility are linked with magnetite. Microcracks grow due to pressure and temperature release during core uplift. This process continues after recovery and is documented by the anelastic strain relaxation and acoustic emissions. The crystalline rocks exhibit marked reversible hydration swelling. Anisotropy of electrical resistivity, permeability, P and S wave velocity is reduced significantly by applying confining pressure, due to closing of microcracks. Fluids within the microcracks also reduce the P wave velocity anisotropy and P wave attenuation. Anisotropy and shear wave splitting observed in the field seismic experiments is caused by the foliation of rocks, as confirmed by laboratory measurements under simulated in situ conditions. The petrophysical studies provide evidence that microfracturing has an important influence on many physical rock properties in situ.
Velocities and Q values of P and S waves as functions of pressure and temperature (at 100 and 600 MPa) are presented for a serpentinite and an amphibolite. Both rocks exhibit a strong lattice preferred orientation (LPO) of the major mineral phases antigorite and hornblende, respectively. Velocities and Q values increase with pressure; the rate of increase is different in the three orthogonal directions (normal and parallel to foliation and lineation) and closely related to progressive closure of microcracks. Increasing temperature decreases velocities and Q values only slightly as long as thermal cracking is prevented by the applied confining pressure. Substantial anisotropy of velocities and Q in P and S waves is observed in both rocks but is found to be different in origin. Anisotropy of P and S wave velocities is highest at low pressure and basically caused by constructive interference of effects related to oriented microcracks and to the LPO of major minerals. Increasing confining pressure decreases velocity anisotropy at a smaller and smaller rate. The residual anisotropy of P and S wave velocities (shear wave splitting) at high confining pressure is mainly a result of preferred mineral orientation. By contrast, anisotropy of Q is very low at low confining pressure and markedly enhanced as pressure is increased. At high confining pressure, substantial anisotropy of Q in P waves is apparent but reversed from that of P wave velocities: Q p is highest in the direction normal to the foliation plane whereas V p (and V S ) is lowest in this direction. The generation of a pronounced anisotropy of Q p by increasing pressure is due to a directionally dependent increase of contact areas on the oriented grain boundaries of the platy minerals defining the foliation. The increase of Q with pressure in the direction normal to foliation is mainly caused by the decrease of energy loss due to compressive strain relative to shear strain. The reverse is true for the X and Y directions (serpentinite) and X direction (amphibolite) parallel to the foliation plane.
Anisotropy of shales is the subject of this report, and we use an example of the Jurassic Opalinus Clay from Mont Terri (Switzerland) that is being investigated in the context of radioactive waste disposal. The study is targeted at the geomechanical characterization of shale by laboratory testing. The overall aim is to improve the constitutive material laws and their application in numerical models.
Abstract Deep underground repositories for radioactive waste generally rely on a multibarrier system to isolate the waste from the biosphere. It consists of the natural geological barrier provided by the repository host rock and its surroundings, the waste container and an engineered barrier system (EBS): that is, the backfilling and sealing of shafts and galleries to block any preferential path for radioactive contaminants. Bentonite emplaced in compacted block form is the preferred option for the clay buffer for most waste management organizations. In assessing the performance of bentonite block masonries, conductive discrete interfaces inside the sealing elements (i.e. contacts between blocks) and to the host rock may act not only as mechanical weakness planes but also as preferential fluid pathways. We performed hydraulic tests on prefabricated bentonite–sand block assemblies (60:40). The results document that despite existing interfaces, the investigated bentonite block assembly behaves no different to that of the homogenous matrix during the saturation of the buffer. This has been confirmed by gas-injection tests on the former interface, as well by shear tests. The outstanding observation is that our results convincingly demonstrate that interfaces between bentonite bricks may ‘heal’ (not only seal), as was physically verified by confirmation of cohesion after presaturation.
Shaft seals are geotechnical barriers in nuclear waste deposits and underground mines. The Sandwich sealing system consists of alternating sealing segments (DS) of bentonite and equipotential segments (ES). MiniSandwich experiments were performed with blended Ca-bentonite (90 mm diameter and 125 mm height) to study hydration, swelling, solute transport and cation exchange during hydration with A3 Pearson water, which resembles pore water of Opalinus Clay Formation at sandy facies. Two experiments were run in parallel with DS installed either in one-layer hydrate state (1W) or in air-dry two-layer hydrate (2W) state. Breakthrough at 0.3 MPa injection pressure occurred after 20 days and the fluid inlet was closed after 543 days, where 4289 mL and 2984 mL, respectively, passed both cells. Final hydraulic permeability was 2.0–2.7 × 10−17 m2. Cells were kept for another 142 days before dismantling. Swelling of DS resulted in slight compaction of ES. No changes in the mineralogy of the DS and ES material despite precipitated halite and sulfates occurred. Overall cation exchange capacity of the DS does not change, maintaining an overall value of 72 ± 2 cmol(+)/kg. Exchangeable Na+ strongly increased while exchangeable Ca2+ decreased. Exchangeable Mg2+ and K+ remained nearly constant. Sodium concentration in the outflow indicated two different exchange processes while the concentration of calcium and magnesium decreased potentially. Concentration of sulfate increased in the outflow, until it reached a constant value and chloride concentration decreased to a minimum before it slightly increased to a constant value. The available data set will be used to adapt numerical models for a mechanism-based description of the observed physical and geochemical processes.
Abstract For the shaft sealing of a repository for radioactive waste, a Sandwich sealing system was developed by KIT-CMM consisting of bentonite-based sealing segments (DS) and sand mixture-based equipotential segments (ES). To demonstrate the functionality of the Sandwich sealing system, various laboratory tests (MiniSandwich tests and semi-technical scale experiments) have been carried out before a large-scale experiment has been implemented in situ at the Mont Terri Rock Laboratory (CH). An important coupled process in the Sandwich system is the swelling deformation of the DS while aqueous fluid penetrates into the system. Consequently, the interparticle porosity (effective porosity) of the DS decreases by swelling strain, resulting in a reduction in the permeability of the DS. Pore space of the ES also decreases slightly due to swelling stress in the adjacent DS, which also leads to a reduction in the permeability of the ES. To understand the coupled hydromechanical processes of the Sandwich sealing system, a numerical model was developed to interpret the experimental observations from the MiniSandwich tests and to parameterize different components. A linear swelling model for DS and empirical functions for the swelling deformation-induced permeability change for both DS and ES segments were introduced into the coupled model with Richards’ flow and elastic model. Sensitivity analysis with parameter variations of the most important parameters reduces the uncertainty in the system behavior.
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