U–Pb zircon age constraints for the Ordovician Fishguard Volcanic Group and further evidence for the provenance of the Stonehenge bluestones
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Abstract:
New U–Pb zircon ages from rhyolite samples of the Fishguard Volcanic Group, SW Wales, confirm a Middle Ordovician (Darriwilian) age for the group. One of the samples is from Craig Rhos-y-felin, which has recently been identified on petrological and geochemical grounds as the source of much of the debitage (struck flakes) at Stonehenge. Analysis of a Stonehenge rhyolite fragment yields an age comparable with that of the Craig Rhos-y-felin sample. Another Stonehenge fragment, thought to come from orthostat (standing stone) 48 and on petrographical grounds to be derived from the Fishguard Volcanic Group (but not Craig Rhos-y-felin), yields an age also consistent with a Fishguard Volcanic Group source. Supplementary material: Details of analytical methods and a table of data are available at https://doi.org/10.6084/m9.figshare.c.3518175 .Detrital zircon U–Pb ages and heavy mineral assemblages provide conflicting evidence of the provenance of the Ordovician–lower Silurian Tumblagooda Sandstone, a fluvial to shallow marine, red-bed succession over 2000 m thick, within the northern Perth and Southern Carnarvon basins in Western Australia. Tourmaline composition indicates a main provenance from interior continental terranes dominated by ‘Li-poor granitoids, pegmatites and aplites’ and ‘Ca-poor metapelites, metapsammites and quartz-tourmaline rocks,’ akin to the Yilgarn Craton to the east of outcrop of the Tumblagooda Sandstone. Other possible source areas include orogens mostly to the south but lack tourmaline analyses for comparison. Taking into account the lack of garnets—a conspicuous component of the adjacent Proterozoic Northampton Inlier—the limited zircon data are compatible with the Albany–Fraser and Pinjarra orogens along the southern and western margins of Australia and/or terranes in or adjacent to East Africa and/or Antarctica, as ultimate source regions with a minor contribution from the Yilgarn Craton, as with other Phanerozoic strata in Western Australia. Whereas the textural and mineralogical maturity of the sandstone could be explained by derivation from such regions, it is more likely that the source was relatively local and that the sediment passed through several phases of reworking. The main source of ilmenite and hematite, by comparison, may have been mafic–ultramafic rocks and/or banded iron formations within the Archean Yilgarn Craton to the east or the Pilbara Craton to the northeast, mobilised by acidic meteoric waters. Iron oxides forming the earliest cements may have been derived from the oxidation of detrital hematite and ilmenite grains concentrated along some bedding laminae or transported in solution from beyond the zone of deposition. Whereas the detrital iron oxides most likely come from the craton to the east of outcrop of the Tumblagooda Sandstone, the sand grains appear to have originally come from a relatively local orogenic source.
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Abstract Single grain zircon U-Pb geochronology has demonstrated great potentials in extracting tectonic and atmospheric circulation signal carried by aeolian, fluvial, and fluviolacustrine sediments. A routine in this sort of studies is analyzing 100–150 grains and then compares zircon U-Pb age spectra between the measured sample and the potential sources. Here we compared the zircon U-Pb age results of the late Miocene-Pliocene Red Clay sequence of two neighboring sites from the Chinese Loess Plateau where similar provenance signal is expected. Although the results from the 5.5 Ma sediment support this prediction, the results from the 3 Ma sediment at these two sites differ from each other significantly. These results emphasize the importance of increasing analysis number per sample and combining the zircon U-Pb geochronology with other provenance tools in order to get reliable provenance information.
Geochronology
Loess plateau
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Abstract Detrital zircon U–Pb geochronology (DZG) is widely used in the provenance analysis and calculating maximum depositional ages (MDAs) of strata. To assess the geologic limitations of this approach, we conducted DZG coupled with bulk‐petrology and heavy‐mineral analyses of Miocene volcaniclastic and non‐volcanic siliciclastic sandstones from the SW Tarim Basin. Although these two sandstone types display greatly different bulk‐petrography and heavy‐mineral signatures, they exhibit similar detrital‐zircon‐age spectra, and thus represent a less common case in which interpretations based on DZG alone may misalign with bulk‐sediment provenance. Most zircon‐based MDAs of volcaniclastic sandstones range from 12.3 to 14.8 Ma, deviating from their ca. 11 Ma true depositional age constrained previously. The similarity of zircon‐age spectra in volcaniclastic and siliciclastic sandstones and the 1–4 M.y. error of the zircon‐based MDAs is ascribed to the low zircon fertility of coeval alkaline magmatic sources. This study emphasizes the importance of an integrated approach to provenance analysis and chronostratigraphy.
Siliciclastic
Geochronology
Paleocurrent
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Sedimentary mineral assemblages commonly contain detrital zircon crystals as part of the heavy-mineral fraction. Age spectra determined by U-Pb isotopic analysis of single zircon crystals within a sample may directly image the age composition—but not the chemical composition—of the source region. Rare earth element (REE) abundances have been measured for zircons from a range of common crustal igneous rock types from different tectonic environments, as well as kimberlite, carbonatite, and high-grade metamorphic rocks, to assess the potential of using zircon REE characteristics to infer the rock types present in sediment source regions. Except for zircon with probable mantle affinities, zircon REE abundances and normalized patterns show little intersample and intrasample variation. To evaluate the actual variation in detrital zircon REE composition in a true sediment of known mixed provenance, zircons from a sandstone sample from the Statfjord Formation (North Sea) were analyzed. Despite a provenance including high-grade metasediment and granitoids and a range in zircon age of 2.82 b.y., the zircon REEs exhibit a narrow abundance range with no systematic differences in pattern shape. These evidences show zircon REE patterns and abundances are generally not useful as indicators of provenance.
Rare-earth element
Carbonatite
Heavy mineral
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Sensitive high-resolution ion microprobe (SHRIMP) U–Pb ages for detrital zircons from the Caspian region reveal the age ranges of basement terrains that supplied the sediment. One sample from the modern Volga river has groupings at c. 340–370 Ma, c. 900–1300 Ma and c. 1450–1800 Ma, with a small number of older zircons. This is consistent with derivation from the Precambrian basement of the East European Craton, and Palaeozoic arcs in the Urals. Mid- and Late Proterozoic components may be derived from beyond the present Volga drainage basin, such as the Sveconorwegian orogen. A Bajocian sandstone from the Greater Caucasus has 73% zircons that post-date 350 Ma. Ages cluster at c. 165–185 Ma, c. 220–260 Ma, c. 280–360 Ma and c. 440–460 Ma. This pattern suggests derivation from Palaeozoic basement of the Greater Caucasus itself and/or the Scythian Platform, and igneous rocks generated at a Jurassic arc in the Lesser Caucasus. Four samples from the Lower Pliocene Productive Series of the South Caspian Basin have common Phanerozoic grains, and groups between c. 900–1300 Ma and 1500–2000 Ma. Each sample contains zircons dated to c. 2700 Ma. The overall age patterns in the Productive Series samples suggest a combination of East European Craton and Greater Caucasus source components.
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Abstract Detrital zircon U-Pb studies of mudstone provenance are rare but may preferentially fingerprint distal zircon sources. To examine this issue, Pierre Shale and Trinidad Sandstone deposited in a Late Cretaceous deltaic environment in the Raton Basin, Colorado (USA), were measured for detrital zircon U-Pb age by laser ablation–inductively coupled plasma–mass spectrometry. Two major detrital zircon age peaks at ca. 70 and 1690 Ma are found in both Pierre Shale and Trinidad Sandstone but in inversely varying proportions: 68% and 16%, respectively, for the finest zircon fraction (~15–35 μm) in the shale, and 25% and 32%, respectively, for the coarsest zircon fraction (~60–80 μm) in the sandstone. Proximal sources in the Sangre de Cristo Mountains, directly west of the Raton Basin, contain coarse-grained, ca. 1690 Ma zircon, whereas distal sources in Laramide uplifts and basins in Colorado, New Mexico, and Arizona contain fine-grained, ca. 70 Ma zircon. The results indicate that U-Pb zircon provenance of mudstone reflects availability of volcanic and other fine-grained source rocks rather than simply distal sources. U-Pb zircon provenance studies should routinely include mudstone units because these units may identify fine-grained zircon sources more reliably than sandstones alone.
Geochronology
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Detrital zircon U-Pb and muscovite 40Ar/39Ar dating are useful tools for investigating sediment provenance and regional tectonic histories. However, the two types of data from same sample do not necessarily give consistent results. Here, we compare published detrital muscovite 40Ar/39Ar and zircon U-Pb ages of modern sands from the Yangtze River to reveal potential factors controlling differences in their provenance age signals. Detrital muscovite 40Ar/39Ar ages of the major tributaries and main trunk suggest that the Dadu River is a dominant sediment contributor to the lower Yangtze. However, detrital zircon data suggest that the Yalong, Dadu, and Min rivers are the most important sediment suppliers. This difference could be caused by combined effects of lower reaches dilution, laser spot location on zircons and difference in closure temperature and durability between muscovite and zircon. The bias caused by sediment laser spot targeting a core or rim of zircon and zircon reworking should be considered in provenance studies.
Muscovite
Thermochronology
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ABSTRACT Detrital-zircon records of provenance are used to reconstruct paleogeography, sediment sources, and tectonic configuration. Recognition of biases in detrital-zircon records that result from grain-size-dependent processes adds new complexity and caution to the interpretation of these records. We begin by investigating possible size-dependent biases that may affect interpretation of detrital-zircon provenance records in an idealized sedimentary system. Our modeling results show that settling and selective entrainment can differentially affect detrital-zircon spectra if an initial size variation between source zircon populations exists. We then consider a case study: a detrital-zircon record from Ediacaran to Terreneuvian strata of Death Valley, USA, with a focus on the Rainstorm Member of the Johnnie Formation. The detrital-zircon record of the Rainstorm Member shows that despite its unusual, heavy-mineral-rich character, the provenance of the unit is like other units in the succession. Size and density measurements of the grains of the deposit suggest that its enriched heavy-mineral suite is best explained through concentration by selective entrainment and winnowing. The relationship between detrital-zircon grain size and age for samples from the Johnnie Formation are consistent with grain-size influence on the interpretation of provenance, especially for large Grenville-age (1.0–1.2 Ga) zircons. Grain size can exert significant bias on a provenance interpretation and must be accounted for in provenance studies.
Heavy mineral
Geologic record
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